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The versatile Premium DSC 204 F1 Phoenix® fascinates with its unique concept: all essential operational components are integrated into the instrument and optional add-ons can be installed anytime on site.
The DSC measuring cell consists of a cylindrical high-conductivity silver block with an embedded heating coil for broad thermal symmetry (3D symmetry) in the sample chamber, the cooling ports for liquid nitrogen or compressed air cooling and a cooling ring for connection of the intracooler (also with simultaneous liquid nitrogen cooling). The gas-tight construction and integrated mass flow controllers for the purge and protective gases allow coupling to an FTIR or MS for gas analysis.
Exchangeable sensors are tailored to their tasks:
With its disk-shaped silver carrier plate and supersensitive thermosensors of nickel-chromium constantan, the Tau-sensor offers a high level of calorimetric sensitivity along with extremely short signal time constants of only 0.6 seconds, which guarantees good separation of overlapping thermal effects.
The µ-sensor stands out for its high level of calorimetric sensitivity, never before achieved with a DSC. For example, it is extremely well suited for pharmaceutical applications with small sample weights.
Important hardware extensions like the automatic sample changer (ASC) for up to 64 sample and reference crucibles, the new UV-extension for photocalorimetry and software features such as BeFlat® for an optimized baseline or the optional temperature modulation of the DSC signal (TM-DSC) make the DSC 204 F1 Phoenix® the most versatile DSC system for R & D, QA, failure analysis and process optimization on the market today.
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COMBINING S/WAXS WITH DSC - A NEW SYSTEM SOLUTION FOR THE LABORATORY
* Absolute SAXS - not a XRD camera with SAXS extension
* Uniquely adaptable SWAXS instrument
* Uniquely embedded CALORIMETER
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DSC 200 F3 Maia® - Differential Scanning Calorimeter
This newest Differential Scanning Calorimeter development at NETZSCH unites compactness, robustness and simple operation with high detection sensitivity for your preferred application in material quality control and failure analysis, especially in polymer processing.
The DSC 200 F3 Maia® combines the advantages of modern technology, high sensitivity and a robust, easy-to-operate work horse. Using liquid nitrogen, the temperature range extends from -170°C to 600°C. The main features of the DSC 200 F3 Maia® are the newly developed monolithic DSC sensor and a new silver furnace with long-life heating element.
The heat flux sensor of the DSC 200 F3 Maia® combines high stability, improved resolution and fast response time. Laser-guided welding processes for the sensor disk and thermocouple wires yield high sensitivity and robustness.
For routine applications we offer the upgrade with an automatic sample changer (ASC) for up to 20 samples and reference materials, also in different crucible types.
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High-sensitivity DSC and microcalorimetry (-45 to 120°C)
Equipped with the exclusive 3D-Sensor Inside Technology, the micro DSC VII is designed principally for the study of substances in a confined environment (denaturation, transition, gelification, reaction, etc.) with rising and falling temperatures (no outside cooling system is needed) and over a wide temperature range (45 to 120°C).
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An-easy-to-use Differential Scanning Calorimeter DSC (-170 to 700°C) with a 3-year warranty
The HIGHLIGHTS
- Robustness: the DSC131 evo features a highly robust sensor that, if needed, can readily be changed by the user in less than 30 minutes. No other DSC offers such flexibility.
- Ease of operation: dedicated market leading CALISTO software that is not only intuitive but powerful enough to perform every typical experiment and data treatment.
- Flexible and powerful: from -170 to 700 °C, with rapid heating and cooling performance.
- Large range of crucibles: in addition to the regular 30 µl crucibles, crucibles with a capacity of 100 µl are used for analyzing heterogeneous samples and for optimizing Cp (heat capacity) measurements.
- High Pressure Crucibles: The High Pressure crucibles deliver unmatched High Pressure resistance (up to 500 bars / 7 250 psi, 600 °C) while the DSC sensor itself remains at atmospheric pressure.
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DSC - Differential Scanning Calorimetry - measures the temperature difference and the heat flow difference between a sample and a reference material (subjected to the same temperature variation in a controlled atmosphere).
DSC determines the temperature and heat of transformation.
MICRO DSC III (-20 to 120°)
Thanks to the exclusive "3D-Sensor Inside" technology, the microcalorimeter Micro DSC III offers very high sensitivity detection for the analysis of liquids, gels, powders, solids, etc.
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Numerous physical processes and chemical reactions are influenced by the surrounding gas pressure. In practise it is therefore often necessary to conduct DSC measurements under an increased pressure.
With the high-pressure DSC 204 HP Phoenix®, thermal effects in a sample can be analyzed in the pressure range from vacuum to 15 MPa (150 bar) and at temperatures from -150°C to 600°C, depending on the type of gas.
The sample chamber atmosphere can be static or dynamic. The electronic pressure monitor and control, along with exact regulation of the purge gas flow, provide for excellent accuracy and reproducibility of the measurement results.
The proven CC 200 L for liquid nitrogen cooling is available for the low-temperature range.
The safety of the high-pressure DSC system has been certified through design tests and is guaranteed during operation by the appropriate safety components.
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An innovative line of Thermal Analyzers (-120 / 830°C) with 3D-Inside technology: DSC, High Pressure DSC, Robot DSC, TG - DSC - coupling to gas analyzer
The HIGHLIGHTS
Incomparable precision: the unique 3D sensor totally surrounds your sample and reference crucibles so that the entire energy of any transformation is monitored thereby giving you an unequalled accuracy of measurement.
Ease of operation: dedicated market leading CALISTO software that is not only intuitive but powerful enough to perform every typical experiments and data treatment.
Parameter Independent Calibration: because of the 3D transducer the calibration of SENSYS evo is independent of:
- mass and form (powder, fibre, liquid, etc.) of the sample,
- contact between the sample and the transducer,
- crucible type,
- sweeping gas (inert, oxidizing, reducing, wet, pressure) and flow rate.
DSC measurement under High Pressure: Two models of sealed "High Pressure"
Crucibles are available in which only the sample and not the sensor is pressurized, thus allowing for the calibration, baseline and sensitivity to remain unchanged.
Large sample volumes: The working volumes of the crucibles (up to 250 μl) are highly suited to the study of heterogeneous samples, or low-energy phase transitions. They are intended for analyses where the pressure generated by the sample remains low. Crucibles are available in alumina, aluminium, rhodiated platinum.
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Mastering High Pressure DSC & Microcalorimetry up to 1000 bars - 14,500 psi
Setaram sells the Gas Hydrates technology UNDER IFP's LICENCE (French Petroleum Industry) PA WO 2006/129018 A2
The microcalorimeter HP microDSC has three main elements:
a highly sensitive microcalorimeter, a pair of special high pressure vessels and a specific Very High Pressure Gas Panel.
The calorimeter is heated and cooled by Peltier elements. The main advantage of this design is that no refrigerating fluid (such as liquid nitrogen) is required to cool the instrument. The minimum temperature that can be reached is 45°C; the maximum is 120°C.
Ultra High Pressure Gas Panel
The pressure inside the sample cell can be controlled by means of a gas panel which can work up to 1000 bar. A pump is used for controlling the pressure inside the cell. It is possible to increase and decrease pressure and to set up some dwell periods. It is also possible to know the gas volume inside the pump and to inject a well defined quantity of gas. Valves are controlled automatically. Pressure can be regulated with an accuracy better than 1%.
The High Pressure Gas Panel has been designed to be used with the highly sensitive microcalorimeter HP micro DSC.
The High Pressure Gas Panel can also be used with other SETARAM systems :
- the innovative Sensys DSC (-120C to 830C) and its 140 l cells
- the low temperature calorimeter BT2.15 (-196 to 200) and its 3.5ml cells
- the Reaction, isothermal and scanning calorimeter C80 (ambient to 300C) with its 3.5ml cells.
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The new DSC 404 F1 Pegasus® by NETZSCH is capable of high precision sample analysis across an extremely broad temperature range from -150°C to 2000°C in a number of applications such as ceramics, metals, plastics, and composites. Unique among high-temperature DSC instruments is the optional temperature-modulated DSC (TM-DSC), which can separate reversible from irreversible energetic effects.
A great variety of both standard and optional features makes the DSC 404 F1 Pegasus® particularly flexible and effective. Various furnaces can be easily interchanged by the user and combined with a swiveling double furnace lifting device. Also, different sample carriers (DSC, DTA), an automatic sample changer (ASC) for up to 20 samples, and plenty of accessories, such as crucibles in numerous shapes and materials, are available.
Its proven vertical format and vacuum-tight construction not only make the DSC 404 F1 Pegasus® easy to operate and very robust, but also enable the implementation of measurements under pure gas atmospheres, which is particularly important for samples sensitive to oxidation. The various DSC sensors are characterized by optimal sensitivity, short response times and high reproducibility.
As with all NETZSCH instruments, this excellent product is complemented by expert application support and first-rate service.
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Large-volume, High-Temperature DSC and (drop) calorimeter (ambient to 1600°C)
The requirements of different experiments are sometimes contradictory, e.g. low sample mass is needed for good transition detection, high sample mass for accurate determination of heat capacity; analysis may need constant or variable temperature; use of the crucible may be open or closed.
Two types of sensor have been developed to meet these different needs.
MHTC 96 hf-dsc for:
- Study of structural transformations in metals and alloys, minerals, oxides.
- Formulation of equilibrium diagrams.
- Study of material reactivity at high temperatures.
- Determination of heat capacity Cp according to the continuous or incremental method.
MHTC 96 drop for:
- In isotherm mode, used especially for drop calorimetry to determine the specific heat of very different materials, the heat of solution of metals in metal baths (alloy formation), oxides in oxide baths (complex oxide formation), calculation of thermal balances, etc.
- In programmed mode, it is the DSC mode for large samples. Applications are analogous to those of the DSC sensor.
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The main advantage of light-curing systems is their fast reaction time. Monomer solutions which are mostly free of solvents can be cured within only a few seconds and already at low temperatures. A combination of thermal and light curing reactions is often applied to dual cure adhesives or paints.
The NETZSCH Photo-DSC 204 F1 Phoenix® works in the temperature range from
-100°C to 200°C. The instrument has a vacuum-tight measuring cell and the purge gas control is regulated by a mass flow controller (MFC).
For our Photo-DSC 204 F1 Phoenix®, most standard industry or laboratory lamps for cationic or radically curing material systems can be used. For the analysis of adhesives, we recommend the DELOLUX04, from the DELO company.
The modified automatic lid-lifting device of the DSC 204 F1 Phoenix® guarantees a defined distance between the two light conductors and the sample and reference.
This achieves high reproducibility of measurement results.
For your normal DSC analyses above 200°C, a retrofit of the standard lid-lifting device is possible, or the manual lid can also be used without problems.
For high sample throughput or for repeat measurements, use of our Automatic Sample Changer (ASC) for up to 64 samples is recommended.
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Pushing the limits of science Our hyper-enabled, double-furnace DSC 8500 is truly revealing
We are proud to introduce you to our DSC 8500. This new double-furnace DSC, features our second-generation HyperDSC® technology. Now you can gain unlimited insight into the structure, properties and performance of your materials and gain the best applications capabilities in the industry. And with our newly designed autosampler, youll be running samples faster then ever before.
Give you laboratory unlimited potential with our DSC 8500.
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The VP-DSC is the most sensitive, easy to use differential scanning calorimeter to study samples in solution. Providing fast, accurate transition midpoint (Tm) determination, the VP-DSC has revolutionized the study of liquid biopharmaceutical formulations by reducing the time and cost of stability testing. In addition, a complete thermodynamic profile is generated to understand the factors that affect conformation and stability.
The VP-DSC is controlled by an intelligent user interface (VPViewer software) and data analysis is performed with Origin®, a market-leading data analysis package.
VP-DSC features:
- Active cell volume ~ 0.5 ml.
- Non-reactive Tantalum 61 cells for excellent chemical resistance.
- Fixed-in-place cells for reproducible ultrasensitive performance with low maintenance.
- Operating temperature range of 10ŗC to +130ŗC.
- Peltier element for precise temperature control.
- User selectable temperature scan rates (0ŗC to 90ŗC per hour upscans) and range for application versatility.
- Unparalleled sensitivity and reproducibility (Figure 1).
- Three user selectable response times (US Patent #5,967,659) for maximum performance.
- Allows studies of fast or slow transition processes.
- Self-contained pressurizing system (0-45 psi) for studying solutions above their boiling point.
- Includes ThermoVac® sample preparation and cleaning device.
- Pressure Perturbation Calorimetry accessory available for the determination of partial specific volumes.
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Thanks to its modular design, the DSC1 as part of the METTLER TOLEDO Thermal Analysis Excellence Line is the best choice for manual or automatic operation, from quality assurance and production through to research and development. The DSC utilizes an innovative patented DSC sensor with 120 thermocouples which guarantees unmatched sensitivity.
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The VP-Capillary DSC System is the most advanced differential scanning calorimeter for screening multiple samples for thermal transition midpoints (Tm). A fully integrated autosampler enables the analysis of up to 50 samples per day with unattended operation. With its advanced capability, the system has revolutionized the study of liquid biopharmaceutical formulations by reducing the time and cost of stability testing.
With higher throughtput and unattended sample handlng capabilities, the VP-Capillary DSC is a powerful tool in drug discovery programs, service laboratories and laboratories screening large numbers of samples. Whether used to screen multiple excipients for formulations or the binding activity of drug compounds against a target, the system can deliver reliable results quickly with minimal operator time.
The VP-Capillary DSC is controlled by an intelligent user interface (VPViewer software) and data analysis is performed with Origin®, a market-leading data analysis package.
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Differential Scanning Calorimeters (DSC) measures temperatures and heat flows associated with thermal transitions in a material. Common usage includes investigation, selection, comparison and end-use performance evaluation of materials in research, quality control and production applications. Properties measured by TA Instruments DSC Differential Scanning Calorimeters techniques include glass transitions, "cold" crystallization, phase changes, melting, crystallization, product stability, cure / cure kinetics, and oxidative stability.
Tzero Differential Scanning Calorimeters TA Instruments' latest development, Tzero DSC Differential Scanning Calorimeters technology, is a revolutionary and fundamentally more accurate way of measuring heat flow. It provides significant improvements in baseline flatness, transition resolution and sensitivity. Tzero Differential Scanning Calorimeters technology allows direct measurement of heat capacity, and makes Modulated® DSC experiments both faster and more accurate. Three DSC modules (Q2000, Q200, Q20) are now available, all significantly advance the DSC Differential Scanning Calorimeters technique to levels previously unattainable.
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STA 449 F1 Jupiter® Simultaneous TG-DSC
Fascinating Flexibility in Thermal Analysis
The new STA 449 F1 Jupiter® combines unlimited configuration flexibility and unmatched performance in just one instruments.
● Thermal stability, decomposition behavior, composition, phase transitions, melting processes to be analyzed comprehensively and quickly
● Easily to use top-loading system with exceptionally precise balance resolution (25 ng resolution at a weighing range of 5g) and highest long-term stability
● Interchangeable sensors for DSC measurements with highest sensitivity and best reproducibility for reaction/transition temperatures and enthalpies as well as for measurements of specific heat
● A variety of optional system enhancements for ideal system adaption to user-defined applications
● Various furnaces, easily interchangeable by the user, available (optional a swiveling double hoisting device for two furnaces)
● Pluggable sample carriers (TG, TG-DSC, TG-DTA, etc.)
● Automatic Sample Changer (ASC) for up to 20 samples
● Automatic evacuation and refilling (Autovac)
● Plenty of accessories, e.g. sample crucibles in the most varied of forms and materials
● Unique for STA: temperature-modulated DSC (TM-DSC)
By supplementary MS-and/or FTIR-coupling even more comprehensive analyzes are possible.
All these features make the new developed STA 449 F1 Jupiter® to the ideal tool for thermal analysis of materials in the fields of research, developments and quality assurance.
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High-performance modular DTA & DSC thermal analyzers (ambient / 2400°C)
SETSYS Evolution DTA up to 2400°C
Highly-sensitive DTA transducers are available:
- A unique tricouple transducer, featuring three thermocouples for the sample and reference sites resulting in unsurpassed sensitivity and resolution; in addition, the detector's symmetry guarantees excellent baseline stability.
- Plate transducer for very-high temperature measurements (up to 2400°C).
- Protected transducer if corrosive gas emanates from the sample.
SETSYS Evolution DSC up to 1600°C
The DSC plate transducer offers an alternative to use of DTA rods.
when a quantitative measurement is desired. It is designed to provide the highest sensitivity over the full temperature range.
Up to 1750°C, platinum, alumina and zirconia crucibles are
proposed for tricouple and protected transducers. Three volumes of crucible (20, 100 and 300 mm3) are available for different masses of sample to be analyzed or thermal effect to be measured. For limited-temperature use (up to 500°C), aluminum crucibles with lids are appropriate for the study of controlled
dehydration.
The DSC plate rod requires the use of flat-bottomed alumina or platinum crucibles. For high temperature or special measurements, tungsten or graphite crucibles with covers are available.
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Simultaneous thermal analysis with maximum efficiency and versatility
STA 409 CD - Simultaneous TG-DSC
The STA 409 CD is based on the classic concept of a thermobalance in a vertically-arranged instrument with top-loaded samples. This design ensures total protection of the digital balance, which is on the bottom, through accurate flow of the purge and protective gases in a natural vertical path to the top, with optimal conditions for coupling FTIR and MS gas analysis systems to the heated furnace outlet. The variety of materials available for components and seals that come into contact with the gases means that measurements are also possible in corrosive gas atmospheres.
Single and double hoist systems for the different types of exchangeable furnaces open up the extremely broad temperature range of -160°C to 2000°C, supported by a multitude of sample carriers and crucibles.
The STA sample carriers are always equipped with a thermocouple for direct measurement of the temperature at the sample/reference crucible (DSC/DTA). There are a number of different thermocouple types to choose from, depending on the application.
The STA 409 CD is designed for simultaneous TG-DSC or simultaneous TG-DTA measurements. The TG sample carriers can be exchanged with TG-DSC or TG-DTA sample carriers in a matter of seconds so that a very powerful and versatile STA is always ready.
When equipped with the Skimmer mass spectrometer coupling, the STA 409 CD becomes the most sophisticated instrument on the market for the analysis of condensable vapors that evolve from a sample at temperatures ranging up to 1450°C or 2000°C.
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Fascinating Flexibility in Thermal Analysis
The new simultaneous thermal analyzer NETZSCH STA 449 F3 Jupiter® allows the measurement of mass changes and thermal effects between -150°C and 2400°C.
The high flexibility caused by the various sensors, the great variety of sample crucibles and the wide TG-measuring range make the system applicable for analysis of all kinds of materials including also inhomogenous substances.
Easily interchangeable sample holders allow the optimal system adaption to the diverse application areas (TG-, TG-DTA- and TG-DSC-measurements).
Various furnaces, easy interchangeable by the user, cover the complete temperature range. (please see accessories)
Through to the vacuum tight design measurements at defined atmospheres (e.g. inert) are possible.
The system is controlled by a newly developed integrated digital electronic device.
The analysis of measuring data runs under a standard PC and the well-proven MS®-WindowsTM software.
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Unrivaled high-temperature TG and DTA performance up to 2400°C with tungsten furnace
The robust STA 429 CD can be equipped with side-mounted motorized hoists for the maximum-temperature 2400°C tungsten furnace or for the Skimmer mass spectrometer coupling. In addition, top-mounted single and double hoisting devices for the different types of exchangeable furnaces provide for an extremely broad temperature range of -160°C to 1700°C.
As with all NETZSCH simultaneous systems, the TG and STA sample carriers are equipped with a thermocouple for direct temperature measurement at the sample/reference crucible. Depending on the temperature range and application, a selection of different thermocouple types is available.
The sample carriers can be exchanged within a matter of seconds so that it is possible to switch between TG and TG-DTA or TG-DSC measurements at any time.
The maximum-temperature TG and TG-DTA sample carriers are made of tungsten in the hot zone and have exchangeable tungsten-rhenium thermocouples. Because measurements are only carried out in pure gas atmospheres or under high vacuum, these proven sample carrier systems have a long service life in spite of the high temperature load.
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An innovative line of Thermal Analyzers (-120 / 830°C) with 3D-Inside technology: DSC, High Pressure DSC, Robot DSC, TG-DSC-coupling to gas analyzer
The HIGHLIGHTS
Differential Scanning Calorimeter
Incomparable precision: the unique 3D DSC sensor totally surrounds your sample and reference crucibles so that the entire energy of any transformation is monitored thereby giving you an unequalled accuracy of measurement.
Parameter Independent Calibration: because of the 3D transducer the calibration of SENSYS evo is independent of:
- mass and form (powder, fibre, liquid, etc.) of the sample,
- contact between the sample and the transducer,
- crucible type,
- sweeping gas (inert, oxidizing, reducing, wet, pressure) and flow rate.
Thermogravimetry
Excellent TG signal baseline: the symmetry of the microbalance, with its sample and reference suspended vertically from the beam guarantee reproducible positioning of the sample over time and excellent stability of the TG signal baseline.
Automatic compensation of Buoyancy: the sample and the reference are heated inside the same calorimetric block (symmetrical furnace), which means that the buoyancy effect is automatically compensated.
Ease of operation: dedicated market leading CALISTO software that is not only intuitive but powerful enough to perform every typical experiments and data treatment.
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TGA, DTA, DSC and Simultaneous TGA-DTA, TGA-DSC from ambient to 1600°C
THE HIGHLIGHTS
- Simplicity of use: thanks to both an ergonomic design and the dedicated market leading Calisto software, LABSYS evo is user friendly and intuitive to operate
- Wide temperature range: TGA with simultaneous DTA or DSC and Cp measurement can be achieved for temperature up to 1 600 °C
- High Precision Cp Measurement: the unique 3D (Calvet type) multiple thermocouples design enables large mass to be measured and to perform a Cp within 2 % , throughout the whole temperature range (ambient 1 600 °C)
- New top loading balance: the unmatched stability, reproducibility and accuracy of this new balance offer unparalleled TGA data
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High-performance modular simultaneous TGA & DTA / DSC thermal analyzer (ambient / 2400°C)
SETSYS Evolution TGA-DTA/DSC: a balance with very high stability and fidelity
SETARAM has brought its extensive experience in the field of balances into play in designing the SETSYS Evolution TGA, a weighing module with exceptional performance. With a maximum capacity of 35 grams the balance is well suited to analysis of samples ranging from microquantities (a few milligrams) to bulky and dense materials, while maintaining a measuring resolution of a microgram whatever the mass analyzed. Of beam and torsion band design, the SETSYS Evolution TGA balance displays great stability, fidelity and sensitivity provided by a high-performance, optical and electronic detection system. The weighing module is robust and made fluid-tight for work under vacuum or with gas scavenging. A version of the balance with a maximum capacity of 100 g is also available.
Simultaneous TGA-DTA/DSC measurements are available using all the different DTA/DSC transducers to cover the following temperature ranges:
Simultaneous TGA-DTA: ambient to 2400°C,
Simultaneous TGA-DSC: ambient to 1600°C.
Coupling with MS, FTIR, GC, etc. gas analyzers by either thermoregulated capillary or the SuperSonic System (sampling by supersonic expansion) for mass spectrometry measurements of up to 1024 amu (heavy and condensable molecules).
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Fascinating Flexibility in Thermal Analysis
DSC 404 F3 Pegasus® - High-Temperature DSC
The new DSC 404 F3 Pegasus® offers a high flexibility for all DSC and DTA applications in quality control and product development. Furnaces and DSC/DTA sensors are available for a broad temperature range (-150...2000°C). Numerous upgrade possibilities allow adaption of this cost-effective system to sophisticated applications.
The DSC 404 F3 Pegasus® is part of the economical NETZSCH F3-product line, which is specially tailored to the requirements of comparative material characterization and quality control.
The DSC 404 F3 Pegasus® can be operated from -150°C to 2000°C with various DTA and DSC sensors that are easily exchangeable by the user and various furnace types.
The sample chamber can be purged with inert or oxidizing gases in order to remove gases evolved from the sample.
The measuring system is vacuum tight (10-2mbar).
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