Process freeze dryer FD-100F-TP

pilotfor the food industryfor the pharmaceutical industry

Short description

• Vaccine freeze dryer rectangular type dry chamber
• Pre-freezing and drying in same chamber without transfer
• 1.15 m2 shelf area, 10kg~15kg/batch, 15kg/24hr ice remove capacity
• High precision thermal oil circulating temperature control method
• Automatic + manual operation, remote control by computer (optional)
• France origin famous brand compressor, circulating pump, pressure gauge
• Air-cooled, no need of external cooling water source
• Suitable for vaccine vials, medicine, IVD, microplate, polypeptide, probiotics, bio samples, food
• CE/ISO9001, conforms to GMP standard, Wall cross design for clean room

Features — Chamber

• Rectangular dry chamber, supports pre-freezing and drying in same chamber without manual transfer
• Drying chamber & shelves made of polished SS304 (SS316 optional for contact parts), high-strength plexiglass observation door, inside round corners for easy cleaning
• Inner wall roughness ≤ 6 μm, shelf flatness ≤ ±0.5 mm/m for best drying performance
• Shelf temperature range: -50°C to +70°C ±1°C (balanced); fast cooling from +20°C to -40°C within 60 min
• Oil circulation heating type with high temperature precision control (suitable for medical/bio); electric heating type available (suitable for food)
• Shelves use safe voltage with controllable heating rate; mirror-polished stainless steel shelves tested for roughness and flatness to ensure uniform temperature
• Wall-cross type available to meet GMP standards

Features — Condenser (cold trap)

• Large-capacity condenser, SS304 construction (SS316 optional for corrosive materials)
• Lowest condenser temperature up to -85°C (silicone oil machine), -60°C for electric heating machine
• Fast cooling from +20°C to -40°C within 30 min
• Independent cylinder-type cold trap with plexiglass door; powerful ice removal capacity
• Patented gas diversion technology for even cold trapping and efficient ice capture
• Electric heating around condenser chamber for effective defrost/ice removal

Features — Refrigeration System

• Dual-stage cooling technology for easier maintenance
• Famous hermetic compressors (e.g., Tecumseh, DANFOSS) for low noise and powerful cooling
• Danfoss brand pressure controller and valve for high stability
• Air-cooled operation without additional cooling device required
• Uses CFC-free, environmentally friendly refrigerant
• Brazed plate heat exchanger

Features — Circulation System

• GUNDFOS (Denmark) shielded circulating pump and PID-controlled electric heating components
• Circulation fluid: low-temperature, low-viscosity silicone oil
• Circulation system applicable for FD-10F-R, FD-20F, FD-30F-TP, FD-50F, FD-100F, FD-200F series

Features — Control System

• Flexible manual + automatic control; manual process setup and automatic batch production modes
• PLC control with 7" LCD touch graphic display (Siemens PLC + 10" touch optional)
• Shelf temperature adjustable and controllable; suitable for pilot and production processes
• 32 programs, each with up to 36 segments; curves can be stored and parameters modified in real time
• Built-in recorder; USB export of data for analysis; FD-LYO software and computer control optional
• Sensor calibration function to ensure long-term measurement accuracy
• Real-time alarm display and historical alarm inquiry for fault diagnosis and maintenance
• User levels and password control for decentralized operation and management
• WIFI remote control via computer or mobile app optional

Features — Vacuum System

• Two-stage rotary vane vacuum pump included (automatic vacuum adjustment and settable)
• Ultimate vacuum up to 1 Pa (higher-end pumps such as LEYBOLD/ULVAC optional)
• Pump performance: atmosphere to 10 Pa in less than 30 min
• System leak rate < 10 Pa·L/sec

Features — Safety Protection

• Comprehensive machine protection and electrical system logic interlocks
• Alarms for vacuum, heating and other system faults
• Power on/off protections and sublimation process safeguards
• Material protection during sublimation; heat cutoff if vacuum is insufficient
• Condenser-vacuum system interlock protection

Features — Others

• Normal type suitable for bulk raw products (food, fruit, herbal medicine, biomaterials)
• Stoppering type suitable for vials with caps; stoppering avoids secondary contamination and moisture re-adsorption
• Inflatable (water) valve with safety diaphragm can be used with inert gas source for inerting and extended shelf life
• CE / ISO9001 / ISO13485 / ISO14001 certificates available; can conform to GMP as per customer requirements

Specifications (table)
FD-100F Series — Model: FD-100F-TP Wall cross design
Heating type: Silicone oil circulation
Drying area: 1.15 m2
Shelf quantity: 4+1 pcs
Shelf temp range: -50°C ~ +70°C ±1°C
Shelf temperature difference: ±1°C (balance)
Shelves size: 480×600 mm
Tray size: 475×595 mm
Tray quantity: 4 pcs
Raw material loaded capacity: 11 L
Height space: 70 mm
Material of chamber: Polish SS304
Material of shelves: Polish SS304
Material of trays: SS304
Vials load capacity (Ф22): 2460 pcs
Vials load capacity (Ф16): 4788 pcs
Vials load capacity (Ф12): 8624 pcs
Condenser temp.: ≤ -85°C
Ice capture capacity: 15 Kg/24h
Defrost: Electric heating
Condenser material: SS304
Vacuum pump: Included
Ultimate vacuum: ≤ 1 Pa
Pump rate: 15 L/s
Style of stoppering: Hydraulic pressure
Cooling type: Air cooled
Dimension (mm): 1640×1105×1635 + 350
Voltage: 3p-380~400V/50Hz
Install Power: 7500 W
Weight: 1000 kg

Technical specifications

• Model: FD-100F-TP
• Heating type: Silicone oil circulation
• Drying area: 1.15 m2
• Shelf quantity: 4+1 pcs
• Shelf temperature range: -50°C to +70°C ±1°C
• Condenser temp.: ≤ -85°C
• Ice capture capacity: 15 kg / 24 h
• Ultimate vacuum: ≤ 1 Pa
• Pump rate: 15 L/s
• Vials capacity examples: Ф22 = 2460 pcs; Ф16 = 4788 pcs; Ф12 = 8624 pcs
• Cooling type: Air-cooled
• Power / Voltage: 7500 W / 3p-380~400V/50Hz
• Dimensions: 1640 × 1105 × 1635 + 350 mm
• Net weight: ~1000 kg
• Materials: Chamber / shelves / trays SS304 (SS316 optional)